HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23113839, compound → HCID 23114211, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23113839 | HCID 23113839 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 23114211 | HCID 23114211 | 65% |
Reaction Steps
Using N-(3-hydroxy-2,2,6,7-tetramethyl-3-(2-thienyl)-2,3-dihydro-1-benzofuran-5-yl)-3,3-dimethylbutanamide obtained in Example 248, the title compound was synthesized in the same manner as in Example 271. Yield: 65%. Melting point: 137-138° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465815B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-fc7e19421692471b88dd53993c2c2fbf |
| Source note | uspto-grants-2008_12 |