HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 86612367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 86612364 | HCID 86612364 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 86612367 | HCID 86612367 | 89% |
Reaction Steps
Using tert-butyl (7-bromo-3-hydroxy-2,2,4,6-tetramethyl-2,3-dihydro-1-benzofuran-5-yl)carbamate obtained in Example 236 and dimethylamine, the title compound was synthesized in the same manner as in Example 297. Yield: 89%. Melting point: 111-112° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465815B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-56f8d1fc42a9482f8cbeca482dcba247 |
| Source note | uspto-grants-2008_12 |