HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 59855627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 1H,1H,5H-Perfluoropentyl acrylate | HCID 67829 | — |
| Product | HCID 59855627 | HCID 59855627 | 97% |
Reaction Steps
With ice cooling and stirring, 9.6 g of morpholine was added dropwise to 28.6 g of 2,2,3,3,4,4,5,5-octafluoropentyl acrylate. The mixture was stirred for one hour at room temperature, after which it was directly distilled for purification. There was obtained 36.2 g of 2,2,3,3,4,4,5,5-octafluoropentyl 3-morpholinopropionate (boiling point 84° C./13 Pa, yield 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07468236B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-ed3846141c464434b958c642eced1352 |
| Source note | uspto-grants-2008_12 |