Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 2-{[(2,2,3,3,4,4,5,5-Octafluoropentyl)oxy]methyl}oxirane | HCID 2775886 | — |
| Product | HCID 58855409 | HCID 58855409 | 89.1% |
Reaction Steps
28.8 g of glycidyl 2,2,3,3,4,4,5,5-octafluoropentyl ether was added dropwise to 8.7 g of morpholine. The mixture was then stirred at 80° C. for 10 hours. The reaction mixture was directly purified by silica gel column chromatography. There was obtained 33.4 g of 1-morpholino-3-(2,2,3,3,4,4,5,5-octafluoropentyloxy)-2-propanol (yield 89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07468236B2 |
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| Source dataset | uspto-grants-2008_12 |
|---|
| ORD ID | ord-2486bcc7ee5744469b72e13b206d08ae |
|---|
| Source note | uspto-grants-2008_12 |
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