HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isonicotinic Acid → Isonicotinoyl chloride hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isonicotinic Acid | HCID 5922 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Isonicotinoyl chloride hydrochloride | HCID 12262826 | — |
Reaction Steps
A solution of isonicotinic acid (0.10 g, 0.8 mmol) and thionyl chloride (1 mL) were heated to reflux for 2 h and concentrated. The product obtained was used immediately in the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07468376B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-5ebf3a2ea9b54de4b354cc2512b07ac4 |
| Source note | uspto-grants-2008_12 |