2-Bromo-1,4-dimethyl-1H-imidazole → 2-(4-Chloro-3,5-dimethyl-phenyl)-1,4-dimethyl-imidazole

Participants

Role	Name	HCID	Charge
Reactant	2-Bromo-1,4-dimethyl-1H-imidazole	HCID 7204877	—
Reactant	2-(4-Chloro-3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane	HCID 53217128	—
Product	2-(4-Chloro-3,5-dimethyl-phenyl)-1,4-dimethyl-imidazole	HCID 86697355	—

Reaction Steps

The title compound is prepared from 2-chloro-1,3-dimethyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzene and 2-bromo-1,4-dimethyl-imidazole following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 7): tR=0.82 min; Mass spectrum (ESI+): m/z=235/237 (Cl) [M+H]+.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08642585B2
Source dataset	uspto-grants-2014_02
ORD ID	ord-59090345900c40afbf00b43cb8603bb5
Source note	uspto-grants-2014_02