HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21099407, compound → HCID 21099405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21099407 | HCID 21099407 | — |
| Reactant | HCID 21099459 | HCID 21099459 | — |
| Product | HCID 21099405 | HCID 21099405 | — |
Reaction Steps
2-chloro-6-[2-(2,4-difluorophenyl)ethyl]-3-(phenylsulfonyl)pyridine and the title compound were prepared from 2-[2-(2,4-difluorophenyl)ethyl]-5-(phenylsulfonyl)pyridine 1-oxide according to the method of Example 29 Step 2, separating the products by dry flash column chromatography using toluene-5% ethyl acetate/toluene. m/z (ES+) 394, 396 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07468393B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-0f0c84d68c53432987d6740428931f39 |
| Source note | uspto-grants-2008_12 |