HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2377047Generated: October 30, 2026
Dimethylformamide dimethyl acetal → HCID 86602114, compound
https://huagongshe.com/reaction/2377047
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | HCID 44549262 | HCID 44549262 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86602114 | HCID 86602114 | — |
Reaction Steps
A mixture of ethyl 4-methyl-5-nitropyridine-2-carboxylate (39.5 g, 0.19 mol), dimethylformamide-dimethylacetal (DMF-DMA) (30.6 g, 0.26 mol, 1.35 eq) in DMF (470 mL) was heated to 90° C. for 30 min. The solvent was removed in vacuo. The residue (78 g) was used without further purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07468375B2 |
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| Source dataset | uspto-grants-2008_12 |
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| ORD ID | ord-b4dc6674623440ea8dd4409b12dd4645 |
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| Source note | uspto-grants-2008_12 |
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