HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → 1-(3-Chloropropyl)-3-(trityloxy)azetidine oxalate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | 1-(3-Chloropropyl)-3-(trityloxy)azetidine | HCID 21990097 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 1-(3-Chloropropyl)-3-(trityloxy)azetidine oxalate | HCID 21990096 | — |
Reaction Steps
In 10 mL of ethyl acetate was dissolved 1-(3-chloropropyl)-3-(trityloxy)azetidine, and to the resulting solution was added 0.15 g of oxalic acid, after which the resulting mixture was stirred at room temperature. The crystals precipitated were collected by filtration to obtain 0.39 g of 1-(3-chloropropyl)-3-(trityloxy)azetidine oxalate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07468443B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-f2632e657b99468e8655f69595147873 |
| Source note | uspto-grants-2008_12 |