HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-methylpropane → Methyl 5-tert-butyl-6-isobutoxy-4'-methyl-3-biphenylcarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-methylpropane | HCID 6555 | — |
| Reactant | Methyl 5-tert-butyl-6-hydroxy-4'-methyl-3-biphenylcarboxylate | HCID 12084822 | — |
| Product | Methyl 5-tert-butyl-6-isobutoxy-4'-methyl-3-biphenylcarboxylate | HCID 12084823 | 95% |
Reaction Steps
In a manner similar to that of Example 1c, by reacting 1.57 g (5.3 mmol) of methyl 5-tert-butyl-6-hydroxy-4′-methyl-3-biphenylcarboxylate with 1.14 mL (10.5 mmol) of isobutyl bromide. A yellow oil is obtained (m=1.8 g; yield=95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07468457B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-ea73c32ded2745508f89479ed511f767 |
| Source note | uspto-grants-2008_12 |