HRID2377616

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10975519

5-Hexenoyl chloride

C6H9ClO

结构：C=CCCCN(C)C(=O)N[C@H](C(=O)O)C(C)(C)C

HCID57431191

3-Methyl-N-[methyl(pent-4-en-1-yl)carbamoyl]-L-valine

C13H24N2O3

PRODUCTS

生成物

结构：C=CCCCCN(C)C(=O)N[C@H](C(=O)O)C(C)(C)C

HCID57431192

N-[(Hex-5-en-1-yl)(methyl)carbamoyl]-3-methyl-L-valine

C14H26N2O3

PROCEDURE

实验过程

3-Methyl-N-{[methyl(hex-5-enyl)amino]carbonyl}-L-valine was prepared according to the procedure for 3-methyl-N-{[methyl(pent-4-enyl)amino]carbonyl}-L-valine (Steps 1-5) by using 5-hexenoyl chloride instead of 4-pentenoyl chloride in Step 1. LRMS (ESI) m/z 271 [(M+H)+; calcd for C14H27N2O3: 271].