HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hexenoyl chloride → N-[(Hex-5-en-1-yl)(methyl)carbamoyl]-3-methyl-L-valine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hexenoyl chloride | HCID 10975519 | — |
| Reactant | 3-Methyl-N-[methyl(pent-4-en-1-yl)carbamoyl]-L-valine | HCID 57431191 | — |
| Product | N-[(Hex-5-en-1-yl)(methyl)carbamoyl]-3-methyl-L-valine | HCID 57431192 | — |
Reaction Steps
3-Methyl-N-{[methyl(hex-5-enyl)amino]carbonyl}-L-valine was prepared according to the procedure for 3-methyl-N-{[methyl(pent-4-enyl)amino]carbonyl}-L-valine (Steps 1-5) by using 5-hexenoyl chloride instead of 4-pentenoyl chloride in Step 1. LRMS (ESI) m/z 271 [(M+H)+; calcd for C14H27N2O3: 271].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07470664B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-1ad30dff3fab40ff956ae072b8b8448e |
| Source note | uspto-grants-2008_12 |