HRID2377626

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID20748

Methyl cyclohexanecarboxylate

C8H14O2

结构：C=CCCC(C)(C)COC(=O)N[C@H](C(=O)O)C(C)(C)C

HCID45379499

N-{[(2,2-Dimethylhex-5-en-1-yl)oxy]carbonyl}-3-methyl-L-valine

C15H27NO4

PRODUCTS

生成物

结构：C=CCCC1(COC(=O)N[C@H](C(=O)O)C(C)(C)C)CCCCC1

HCID45379503

N-({[1-(But-3-en-1-yl)cyclohexyl]methoxy}carbonyl)-3-methyl-L-valine

C18H31NO4

PROCEDURE

实验过程

N-{[(1-But-3-en-1-ylcyclohexyl)methoxy]carbonyl}-3-methyl-L-valine was prepared according to the procedure for N-{[(2,2-dimethylhex-5-enyl)oxy]carbonyl}-3-methyl-L-valine by using methyl cyclohexanecarboxylate instead of ethyl isobutyrate in Step 1. LRMS (ESI) m/z 326.3 [(M+H)+; calcd for C18H32NO4: 326.2].