Methyl cyclohexanecarboxylate → N-({[1-(But-3-en-1-yl)cyclohexyl]methoxy}carbonyl)-3-methyl-L-valine

Participants

Role	Name	HCID	Charge
Reactant	Methyl cyclohexanecarboxylate	HCID 20748	—
Reactant	(S)-2-((((2,2-Dimethylhex-5-en-1-yl)oxy)carbonyl)amino)-3,3-dimethylbutanoic acid	HCID 45379499	—
Product	N-({[1-(But-3-en-1-yl)cyclohexyl]methoxy}carbonyl)-3-methyl-L-valine	HCID 45379503	—

Reaction Steps

N-{[(1-But-3-en-1-ylcyclohexyl)methoxy]carbonyl}-3-methyl-L-valine was prepared according to the procedure for N-{[(2,2-dimethylhex-5-enyl)oxy]carbonyl}-3-methyl-L-valine by using methyl cyclohexanecarboxylate instead of ethyl isobutyrate in Step 1. LRMS (ESI) m/z 326.3 [(M+H)+; calcd for C18H32NO4: 326.2].

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07470664B2
Source dataset	uspto-grants-2008_12
ORD ID	ord-cd60d2e607b8452ab847e7845ad4f6b9
Source note	uspto-grants-2008_12