Propylamine → 3-Methyl-N-[(pent-4-en-1-yl)(propyl)carbamoyl]-L-valine

HRID 2377643Notes

Reaction equation

HRID 2377643 reaction equation
[CH:1]([N:4]([CH2:16][CH2:17][CH2:18][CH:19]=[CH2:20])[C:5]([NH:7][C@H:8]([C:13]([OH:15])=[O:14])[C:9]([CH3:12])([CH3:11])[CH3:10])=[O:6])([CH3:3])C.[CH2:21](N)CC>>[CH3:12][C:9]([CH3:10])([CH3:11])[C@@H:8]([C:13]([OH:15])=[O:14])[NH:7][C:5]([N:4]([CH2:16][CH2:17][CH2:18][CH:19]=[CH2:20])[CH2:1][CH2:3][CH3:21])=[O:6]

Participants

3

Reactant 2

HCID 7852PropylamineHCID 576926803-Methyl-N-[(pent-4-en-1-yl)(propan-2-yl)carbamoyl]-L-valine

Product 1

HCID 574311983-Methyl-N-[(pent-4-en-1-yl)(propyl)carbamoyl]-L-valine

Procedure

3-Methyl-N-{[pent-4-en-1-yl(propyl)amino]carbonyl}-L-valine was prepared according to the procedure described for N-{[isopropyl(pent-4-en-1-yl)amino]carbonyl}-3-methyl-L-valine by using n-propylamine in Step 1. LRMS (ESI) m/z 285 [(M+H)+; calcd for C15H29N2O3: 285.2].

Sources & evidence

ORD record
ord-d74596c74e3b4cfd8f080c5a3be8fc4d
Source dataset
uspto-grants-2008_12
Patent number
US07470664B2

Reaction notes

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