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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 237767Generated: October 30, 2026

HCID 68527500, compound → HCID 45788691, compound

https://huagongshe.com/reaction/237767

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68527500HCID 68527500—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 45788691HCID 45788691—

Reaction Steps

To a solution of 6-cyclohex-1-enyl-pyridin-3-ol (2.2 g, 12.6 mmol) in methanol (45 ml) was added 10% Pd/C (0.22 g) under N2. This mixture was stirred under hydrogen (1 atm) for 3 h. The reaction mixture was filtered through celite. The filtrate was concentrated to a solid (2.2 g) to provide the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08642603B2
Source datasetuspto-grants-2014_02
ORD IDord-1bec961635104b7bbd9212609fd497ce
Source noteuspto-grants-2014_02