HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 11325467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 4-Nitro-1,2-phenylenediamine | HCID 5111791 | — |
| Reactant | HCID 86611513 | HCID 86611513 | — |
| Product | HCID 11325467 | HCID 11325467 | — |
Reaction Steps
For further reaction, 1006 mg of 4-nitro-1,2-phenylenediamine and 150 mg of the thioisocyanate 3 prepared are dissolved in 5 ml of dimethylformamide and stirred overnight at room temperature. After removal of the solvent, the residue was purified by MPLC chromatography (Rp 18), giving 126 mg of benzimidazolamine 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07470702B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-41a87740575442d88f823289f5b836c9 |
| Source note | uspto-grants-2008_12 |