HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2378085Generated: October 30, 2026
3-Hydroxypiperidine → HCID 67268684, compound
https://huagongshe.com/reaction/2378085
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Hydroxypiperidine | HCID 23293 | — |
| Reactant | HCID 67268920 | HCID 67268920 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67268684 | HCID 67268684 | — |
Reaction Steps
A mixture of 0.12 g 5-(3-methyl-but-2-enyl)amino-[1,3,4]oxadiazole-2-carboxylic acid-(naphth-1-ylmethyl)-amide and 1.80 g 3-hydroxypiperidine is stirred for 20 min at 200° C. in a microwave. After cooling to ambient temperature dichloromethane is added, the organic phase is washed once with water and once with 1 M hydrochloric acid, dried over sodium sulphate, and the solvent is removed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07470716B2 |
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| Source dataset | uspto-grants-2008_12 |
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| ORD ID | ord-a19fb9cb65e946b3b8951582459a01bd |
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| Source note | uspto-grants-2008_12 |
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