Acetic Acid → HCID 69277781, compound

Participants

Reaction Conditions

Reaction Steps

To a 15 ml of acetic acid solution of 2.23 g of 4-(4-trifluoromethylbenzylsulfanyl)phenol was added slowly, 2.5 ml of 30% hydrogen peroxide solution at approximately 80° C. The reaction mixture was stirred for 3 hours at 90° C., then poured into water, and the resulted precipitate was collected by filteration. After washing with water, the precipitate was dried by heating under the reduced pressure to produce 2.34 g of the desired product.

Provenance & Evidence