HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl 3-(3-fluoro-4-methyloxyphenyl)Acrylate → HCID 22558762, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl 3-(3-fluoro-4-methyloxyphenyl)Acrylate | HCID 53705486 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | HCID 22558762 | HCID 22558762 | 99,4% |
Reaktionsschritte
A solution of Intermediate 7 (3.01 g) in ethyl acetate (50 ml) and methanol (25 ml) was added with 10% palladium/carbon (300 mg, Merck), and stirred at room temperature for 2 hours under hydrogen atmosphere. The reaction mixture was filtered, and the solvent of the filtrate was evaporated under reduced pressure to obtain the title compound (Intermediate 8, 3.02 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07470807B2 |
| Quelldatensatz | uspto-grants-2008_12 |
| ORD ID | ord-3cec7341f3274df9a0847e009ebb01c9 |
| Quellennotiz | uspto-grants-2008_12 |