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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2378530Erstellt: 26. Oktober 2026

Ethyl 3-(3-fluoro-4-methyloxyphenyl)Acrylate → HCID 22558762, Verbindung

https://huagongshe.com/reaction/2378530

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthyl 3-(3-fluoro-4-methyloxyphenyl)AcrylateHCID 53705486—
KatalysatorPalladiumHCID 23938—
LösungsmittelMethanolHCID 887—
LösungsmittelEthyl AcetateHCID 8857—
ProduktHCID 22558762HCID 2255876299,4%

Reaktionsschritte

A solution of Intermediate 7 (3.01 g) in ethyl acetate (50 ml) and methanol (25 ml) was added with 10% palladium/carbon (300 mg, Merck), and stirred at room temperature for 2 hours under hydrogen atmosphere. The reaction mixture was filtered, and the solvent of the filtrate was evaporated under reduced pressure to obtain the title compound (Intermediate 8, 3.02 g).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07470807B2
Quelldatensatzuspto-grants-2008_12
ORD IDord-3cec7341f3274df9a0847e009ebb01c9
Quellennotizuspto-grants-2008_12