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HRID2378545

反应详情

EQUATION

反应方程式

HRID 2378545 的结构方程式

REACTANTS

反应物

3
结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：COc1ccc(CCC(=O)O)cc1F
HCID3017966

3-(3-Fluoro-4-methoxyphenyl)propanoic acid

C10H11FO3

结构：COC(=O)CCc1cc(-c2ccc3ccccc3c2)c(OC)c([N+](=O)[O-])c1
HCID22558707

未命名化合物

PRODUCTS

生成物

1
结构：COc1c(-c2ccc3ccccc3c2)cc(CCC(=O)O)cc1[N+](=O)[O-]
HCID22559188

未命名化合物

收率 83.2%

PROCEDURE

实验过程

According to the procedure described in the synthesis method of Intermediate 9 provided that the reaction was carried out for 40 minutes, Intermediate 49 (2.45 g) and 2 N aqueous sodium hydroxide (6.7 ml) were reacted and treated to obtain the title compound (Intermediate 60, 1.96 g).

WORKUP

后处理

  1. customprovided that the reaction
  2. additiontreated