HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → 4-Phenylsulfanyl-but-2-ynoic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Phenyl propargyl sulfide | HCID 4131667 | — |
| Product | 4-Phenylsulfanyl-but-2-ynoic acid ethyl ester | HCID 68529379 | — |
Reaction Steps
The title compound was prepared from prop-2-ynylsulfanyl-benzene and ethyl chloroformate in accordance with the procedures of G. Cai et al., Tetrahedron, 2006, (5697-5708).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642603B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-68705773253f4cab8a46b226b3a070a2 |
| Source note | uspto-grants-2014_02 |