HCID 178463917, compound → HCID 178438921, compound

HRID 2379019Notes

Reaction equation

HRID 2379019 reaction equation
C(N(C[C:7]1[CH:12]=[C:11]([C:13]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)([CH3:15])[CH3:14])[CH:10]=[C:9]([C:22]2[C:30]3[N:29]=[N:28][NH:27][C:26]=3[CH:25]=[CH:24][CH:23]=2)[C:8]=1[OH:31])CC)C>C1(C)C(C)=CC=CC=1>[C:13]([C:11]1[CH:10]=[C:9]([C:22]2[C:30]3[N:29]=[N:28][NH:27][C:26]=3[CH:25]=[CH:24][CH:23]=2)[C:8]([OH:31])=[CH:7][CH:12]=1)([C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1)([CH3:15])[CH3:14]

Participants

3

Reactant 1

HCID 178463917HCID 178463917, compound

Product 1

HCID 178438921HCID 178438921, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

The xylene solution was prepared in the same manner as in Synthesis Example (10) except that there were used 10.0 g of 2-diethylaminomethyl-4-cumyl-6-benzotriazolylphenol or a Mannich base compound, which had been obtained in the same manner as in Synthesis Example (10), except that 4-cumyl-6-benzotriazolylphenol was used as the main material for the Mannich base compound, and 6.6 g of 4-cumyl-6-benzotriazolylphenol. The resulting solution was allowed to react in the same manner as in Synthesis Example (10) and subjected to the same treatment as in Synthesis Example (10) to obtain an opal crystal having a melting point of 191° C. (the intended product).

Sources & evidence

ORD record
ord-076909790f9b4b6c9e91abb35d7f3ca6
Source dataset
uspto-grants-1994_11
Patent number
US05360692

Reaction notes

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