HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethyl ethyl ether → 1-(2-Ethoxyethyl)-4-cyano-4-phenyl-piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethyl ethyl ether | HCID 61141 | — |
| Reactant | 4-Piperidinecarbonitrile, 4-phenyl- | HCID 181138 | — |
| Product | 1-(2-Ethoxyethyl)-4-cyano-4-phenyl-piperidine | HCID 18957813 | — |
Reaction Steps
The title compound was prepared as described in Example I 2 from 4-cyano-4-phenylpiperidine and 2-bromoethyl ethyl ether excluding KI: Reaction time under reflux 6 hours. The compound boiled at 130°-135°/0.005 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05360805 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-81ecb32af180451fae4732884ef92266 |
| Source note | uspto-grants-1994_11 |