Water → HCID 15616312, compound

Participants

Reaction Steps

Sodium borohydride (139 mg) was added to a stirred solution of 4-formyl-N,N-dimethyl-5-propyl-1H-imidazole-1-sulphonamide (450 mg) in absolute ethanol (5 ml) under nitrogen. After 3 h the mixture was poured into water (30 ml) and extracted with dichloromethane (3×15 ml). The combined, dried organic extracts were evaporated to give a solid (425 mg) which was triturated with ether (2×10 ml) to give the title compound (350 mg), m.p. 86°-88°.

Provenance & Evidence