HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 9838760, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-[3-(2-Amino-1-hydroxyethyl)-4-fluorophenyl]methanesulfonamide | HCID 9838761 | — |
| Product | HCID 9838760 | HCID 9838760 | — |
Reaction Steps
(±)-3'-(2-Amino-1-hydroxyethyl)-4'-fluoromethanesulfonanilide (2.3 g) was treated with 20% ethanolic hydrochloric acid to give 2.4 g of (±)-3'-(2-amino-1-hydroxyethyl)-4'-fluoromethanesulfonanilide hydrochloride, m.p. 178°-181° C. Elementary analysis for C9H13FN2O3S.HCl. Calcd: C 37.96, H 4.96, N 9.84; Found: C 37.97, H 5.06, N 9.59.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05360822 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-008a1a7aecfd432ab6ca84e7a14ec9f2 |
| Source note | uspto-grants-1994_11 |