HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenol → HCID 12311537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenol | HCID 7808 | — |
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Product | HCID 12311537 | HCID 12311537 | 63% |
Reaction Steps
Analogous to Example 1, p-bromophenol was reacted with cyanogen bromide to obtain the title compound as white crystals. The yield was 63% of theory. The product was identified by its NMR spectrum as well as by the absorption of the cyanato group at 2260 cm-1 and the absence of phenolic hydroxy absorption in the IR spectrum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05360887 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-4a9b02bb70eb4781bdf2be5d07edb0d7 |
| Source note | uspto-grants-1994_11 |