4-Bromophenol → HCID 12311537, compound

HRID 2379244Notes

Reaction equation

HRID 2379244 reaction equation
[CH:1]1[C:6]([OH:7])=[CH:5][CH:4]=[C:3]([Br:8])[CH:2]=1.[N:9]#[C:10]Br>>[Br:8][C:3]1[CH:4]=[CH:5][C:6]([O:7][C:10]#[N:9])=[CH:1][CH:2]=1

Participants

3

Reactant 2

HCID 78084-BromophenolHCID 10476Cyanogen Bromide

Product 1

HCID 12311537HCID 12311537, compoundYield 63%

Procedure

Analogous to Example 1, p-bromophenol was reacted with cyanogen bromide to obtain the title compound as white crystals. The yield was 63% of theory. The product was identified by its NMR spectrum as well as by the absorption of the cyanato group at 2260 cm-1 and the absence of phenolic hydroxy absorption in the IR spectrum.

Sources & evidence

ORD record
ord-4a9b02bb70eb4781bdf2be5d07edb0d7
Source dataset
uspto-grants-1994_11
Patent number
US05360887

Reaction notes

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