反应详情

β-D-galactose (10 g, 1 eq), decylamine (8.7 g, 1 eq), and water (2 g, 3eq) were heated in a reaction flask for 20 min at 80° C. Methanol/ethyl ether (50 v/50 v) was added, the product was filtered, washed with ethyl ether (2×50 ml) and dried, to give a 90% yield.

1. filtrationthe product was filtered
2. washwashed with ethyl ether (2×50 ml)
3. customdried
4. customto give a 90% yield