HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 11070066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 1,1,1-Tris(4-hydroxyphenyl)ethane | HCID 93118 | — |
| Reactant | Acetone-D6 | HCID 522220 | — |
| Product | HCID 11070066 | HCID 11070066 | 97% |
Reaction Steps
1,1,1-Tris(4-hydroxyphenyl)ethane was acetylated with acetic anhydride as in the example above. A white solid was obtained in 97% yield, MP=169° C. NMR (1H, d-6 acetone)--7.06(q), 2.28(s), 2.24(s), 13C NMR (d-6 acetone)--169.65, 149, 146.19, 129.75, 120.98, 51.45, 30.61, 20.91.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05362843 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-df34ef33f6184a0aaa3e0c36bcb26e90 |
| Source note | uspto-grants-1994_11 |