HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4'-Decyloxybiphenyl-4-carboxylic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4'-Decyloxybiphenyl-4-carboxylic Acid | HCID 11451085 | — |
| Product | 4'-Decyloxybiphenyl-4-carboxylic acid chloride | HCID 14069944 | — |
Reaction Steps
4'-n-Decyloxy-4-carboxybiphenyl (3.00 g) was heated under reflux for 6 hours together with an excessive amount of thionyl chloride, and the unaltered thionyl chloride was removed by distillation to give about 3 g of 4'-n-decyloxybiphenyl-4-carboxylic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05364561 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-27266cd6d2d84f0f9f4444d5fe196321 |
| Source note | uspto-grants-1994_11 |