HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-(4-Octyloxyphenyl)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4'-(Octyloxy)-[1,1'-biphenyl]-4-carboxylic acid | HCID 2802556 | — |
| Product | 4-(4-Octyloxyphenyl)benzoyl chloride | HCID 11078473 | — |
Reaction Steps
After 4-n-octyloxybiphenyl-4'-carboxylic acid (3.0 g) was heated under reflux together with an excessive amount of thionyl chloride for 6 hours, unaltered thionyl chloride was removed by distillation to give 4-n-octyloxybiphenyl-4'-carboxylic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05364561 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-f183556b988f4894adc97b5487279cc8 |
| Source note | uspto-grants-1994_11 |