Benzylamine → HCID 18757511, compound

Participants

Reaction Steps

The above compound (3) (1.1 g) was dissolved in 30 ml of ethanol, and 3 g of benzylamine was added dropwise. The mixture was stirred at room temperature for 24 hours, then diluted with 300 ml of ether, washed with dilute hydrochloric acid and water in this sequence, and dried over magnesium sulfate. After the solvent was evaporated, the solid was purified by silica gel column chromatograhy to afford 0.6 g of a final product (4).

Provenance & Evidence