HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromochloromethane → HCID 18956522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromochloromethane | HCID 6333 | — |
| Reactant | HCID 18956523 | HCID 18956523 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 18956522 | HCID 18956522 | 56.8% |
Reaction Steps
Treatment of the product of part (ii) (2.0 g) with bromochloromethane (1.15 g) and n-butyllithium (5.28 ml of a 1.6M solution in hexane) according to the method of Example 11(iii) gave the title compound as a gum (1.20 g) which was used directly in the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05364938 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-111926274c414aa99d64d4644270f641 |
| Source note | uspto-grants-1994_11 |