HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromochloromethane → HCID 18956528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromochloromethane | HCID 6333 | — |
| Reactant | HCID 18956533 | HCID 18956533 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Reactant | HCID 178506875 | HCID 178506875 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 18956528 | HCID 18956528 | — |
Reaction Steps
Treatment of the product of part (ii) (3.10 g) with chloromethyllithium (prepared from bromochloromethane (1.78 g) and a 1.6M solution of n-butyllithium in hexane (8.20 ml)) according to the method of Example 11(iii) gave the title compound as a gun (2.25 g), which was used directly in the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05364938 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-84289e22fabc4ec59a765bb60e0a8eeb |
| Source note | uspto-grants-1994_11 |