HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 15219348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Chloro-3-ethyl-1-methyl-1H-pyrazole-5-carbonyl chloride | HCID 45081914 | — |
| Reactant | HCID 86748271 | HCID 86748271 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15219348 | HCID 15219348 | — |
Reaction Steps
A mixture consisting of 2 ml of methylene chloride, 0.11 ml of triethylamine and 250 mg of 3-chloro-4-((2-trifluoromethoxy-1,1,2-trifluoroethoxy)-benzylamine (0.77 moles) is slowly added dropwise to a solution of 166 mg (0.8 mmoles) of 4-chloro-3-ethyl-1-methyl-5-pyrazolecarboxylic acid chloride in 3 ml of methylene chloride. The solution obtained is maintained under agitation at ambient temperature for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05366991 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-2eccc92e1836406e9facd96dfab536a4 |
| Source note | uspto-grants-1994_11 |