HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 53841370, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Chloro-3-ethyl-1-methyl-1H-pyrazole-5-carbonyl chloride | HCID 45081914 | — |
| Reactant | HCID 86748271 | HCID 86748271 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53841370 | HCID 53841370 | — |
Reaction Steps
A mixture consisting of 4 ml of methylene chloride, 0.22 ml of triethylamine and 450 mg of 4-((2-trifluoromethoxy-1,1,2-trifluoroethoxy)-benzylamine (1.56 moles) is slowly added dropwise to a solution of 332 mg (1.6 mmoles) of 4-chloro-3-ethyl-1-methyl-5-pyrazolecarboxylic acid chloride in 6 ml of methylene chloride. The solution obtained is maintained under agitation at ambient temperature for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05366991 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-6ad40c4235724cd3852d578898d81882 |
| Source note | uspto-grants-1994_11 |