HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24866633, compound → HCID 178424208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24866633 | HCID 24866633 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178424208 | HCID 178424208 | — |
Reaction Steps
1-tert-butyl-3-o-tolyl-1H-pyrazolo[3,4-d]pyrimidin-4-amine was dissolved in a solution of formic acid (2 mL) and conc. HCl (0.2 mL) and heated to reflux for 30 min. Reaction was concentrated in vacuo and purified by RP-HPLC (MeCN:H2O:0.1% TFA). ESI-MS (M+H)+ m/z calcd 226.1, found 226.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642604B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-812cd83691384435bea30c2c05e006c7 |
| Source note | uspto-grants-2014_02 |