反应详情

温度

110 °C

4-chloro-5-iodo-7-methyl-7H-pyrrolo[2,3-d]pyrimidine (90 mg, 0.31 mmol) was taken up in 7N NH3/MeOH and heated in a sealed tube at 110° C. overnight. Reaction was concentrated in vacuo to give a brown/off-white solid.

1. customReaction
2. concentrationwas concentrated in vacuo
3. customto give a brown/off-white solid