Methyl iodide → HCID 18954835, compound

Participants

Reaction Steps

A mixture of 0.54 g of the compound from Step C and 0.1 mL of iodomethane were stirred overnight after which time the precipitated solids were filtered and dried. This product was suspended in 2 mL of chloroform and 2 mL of 5% aqueous sodium bicarbonate was added. After stirring overnight the layers were separated and the chloroform extracts dried over magnesium sulfate and concentrated to afford 0.12 g of the title compound as a yellow oil.

Provenance & Evidence