HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycylglycine → Methacryloylglycylglycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycylglycine | HCID 11163 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Solvent | Water | HCID 962 | — |
| Product | Methacryloylglycylglycine | HCID 10241886 | 75% |
Reaction Steps
Using Example 1, glycylglycine was reacted with methacryloyl chloride in water at -10° C. After adjustment to a pH of 3, the white slurry was washed with ethanol to remove sodium chloride and water. The product was dried at 80° C. to obtain a good yield (>75%) product with a melting point of 200°-201° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05369142 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-86af07b8d12f4df8a95f65f97388eba5 |
| Source note | uspto-grants-1994_11 |