反应详情

Using Example 1, glycylglycine was reacted with methacryloyl chloride in water at -10° C. After adjustment to a pH of 3, the white slurry was washed with ethanol to remove sodium chloride and water. The product was dried at 80° C. to obtain a good yield (>75%) product with a melting point of 200°-201° C.

1. washAfter adjustment to a pH of 3, the white slurry was washed with ethanol
2. customto remove sodium chloride and water
3. customThe product was dried at 80° C.
4. customto obtain