HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 59364049, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Potassium bisulfate | HCID 516920 | — |
| Reactant | HCID 59364042 | HCID 59364042 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 59364049 | HCID 59364049 | — |
Reaction Steps
To a solution of 2-Benzyl-3-(4-phenyl-thiazol-2-ylamino)-propionic ethyl ester (22r) (0.028 mmol, 10 mg) in EtOH (2 mL) and water (200 μL) is added KOH 1N solution (224 μL, 8 eq.). After 5 hours, the solution is neutralized with KHSO4 1N solution and lyophilized before purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08257931B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-80affb7eb23e4bd3842fa7721b6694e5 |
| Source note | uspto-grants-2012_09 |