HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2,2,2-Trifluoro-1-methyl-ethoxy)-aniline → HCID 51001322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2,2,2-Trifluoro-1-methyl-ethoxy)-aniline | HCID 66277568 | — |
| Reactant | 4-Fluoro-1-(toluene-4-sulfonyl)-piperidine-4-carboxylic acid | HCID 69810320 | — |
| Product | HCID 51001322 | HCID 51001322 | 10.3% |
Reaction Steps
This material was made in analogy to example 1 from 4-fluoro-1-(toluene-4-sulfonyl)-piperidine-4-carboxylic acid (0.15 g), (rac)-4-(2,2,2-trifluoro-1-methyl-ethoxy)-phenylamine (0.102 g) to give the desired (rac)-4-fluoro-1-(toluene-4-sulfonyl)-piperidine-4-carboxylic acid [4-(2,2,2-trifluoro-1-methyl-ethoxy)-phenyl]-amide (0.025 g) as an off-white solid. MS (ESI): 489.25 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08258158B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-95ec9cf301794bea81b3594e7964673f |
| Source note | uspto-grants-2012_09 |