Sodium Iodide → HCID 24781135, compound

HRID 2381583Notes

Reaction equation

HRID 2381583 reaction equation
[CH3:1][C:2]([O:7][C:8]1[CH:13]=[CH:12][C:11]([CH:14]=[CH:15][C:16](=[O:27])[C:17]2[CH:22]=[CH:21][C:20]([S:23][CH2:24][CH2:25][CH3:26])=[CH:19][CH:18]=2)=[CH:10][C:9]=1[CH3:28])([CH3:6])[C:3]([OH:5])=[O:4].[I-].[Na+].Cl[Si](Cl)(Cl)Cl>>[CH3:28][C:9]1[CH:10]=[C:11]([CH2:14][CH2:15][C:16]([C:17]2[CH:22]=[CH:21][C:20]([S:23][CH2:24][CH2:25][CH3:26])=[CH:19][CH:18]=2)=[O:27])[CH:12]=[CH:13][C:8]=1[O:7][C:2]([CH3:6])([CH3:1])[C:3]([OH:5])=[O:4]

Participants

4

Reactant 3

HCID 5238Sodium IodideHCID 24816Silicon tetrachlorideHCID 86654221HCID 86654221, compound

Product 1

HCID 24781135HCID 24781135, compound

Procedure

This compound was prepared following the general procedure B, using 2-methyl-2-(2-methyl-4-(3-oxo-3-(4-(propylthio)phenyl)prop-1-enyl)phenoxy)propanoic acid tertiobutyl ester, and 3 equivalents amounts of sodium iodide and 3 equivalent amounts of tetrachlorosilane;

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-67d92550f3f1449b9f58c70fa72b964f
Source dataset
uspto-grants-2012_09
Patent number
US08258182B2

Reaction notes

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