HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59179696, compound → HCID 59179651, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59179696 | HCID 59179696 | — |
| Reactant | HCID 68493040 | HCID 68493040 | — |
| Product | HCID 59179651 | HCID 59179651 | 70% |
Reaction Steps
Following the procedure as described in Example 13, making variations as necessary to replace ethyl 4-methyl-2-(4-(3-phenylpropyl)-1H-1,2,3-triazol-1-yl)thiazole-5-carboxylate with ethyl 4-methyl-2-(4-(2-phenylpropyl)-1H-1,2,3-triazol-1-yl)thiazole-5-carboxylate, the title compound was obtained as a white solid in 70% yield: 1H NMR (300 MHz, CDCl3) δ 11.21 (s, 1H), 8.08 (s, 1H), 7.31-7.21 (m, 5H), 3.19-3.05 (m, 4H), 2.75 (s, 3H); MS (ES+) m/z 315.3 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08258160B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-5c4ad7ef8cce4ea1809a1114bca6884c |
| Source note | uspto-grants-2012_09 |