HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 2-aminoacetate hydrochloride → HCID 131729934, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 2-aminoacetate hydrochloride | HCID 11701227 | — |
| Reactant | HCID 178453398 | HCID 178453398 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131729934 | HCID 131729934 | 105% |
Reaction Steps
To a magnetically stirred solution of H-Gly-OBn.HCl (2.50 g, 12.4 mmol) in DMF (80 ml) was added TEA (4.4 ml, 31.0 mmol) followed by PNPO-Lys(Boc)2 (6.96 g, 14.9 mmol). The reaction and product isolation were carried out according to the method of Example 72.i to give BnO-GlyLys[Boc]2 as a pale yellow foam (6.42 g, 105%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08258259B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-05def70a594f4321a1a41c7762dd1350 |
| Source note | uspto-grants-2012_09 |