HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl orthoformate → HCID 178424340, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | N-Phenanthridin-6-yl-N'-o-tolylhydrazine hydrochloride | HCID 67128317 | — |
| Product | HCID 178424340 | HCID 178424340 | — |
Reaction Steps
A suspension of N-phenanthridin-6-yl-N′-o-tolylhydrazine hydrochloride (9.0 g, 27 mmol) in triethyl orthoformate (360 ml) is stirred under reflux under argon for 17 h. After cooling to room temperature, the precipitate is filtered off and washed with triethyl orthoformate and cold acetone. Yield: 8.2 g (88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08258297B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-7f88bf9d27db475fb9f264afa88ff6da |
| Source note | uspto-grants-2012_09 |