Benzenepropanal → HCID 25122340, compound

Participants

Reaction Steps

Compound 11 was prepared as described for compound 9, using 3-phenylpropionaldehyde in place of benzaldehyde. 1H NMR (CD3OD, 400 MHz) δ 8.20 (d, 1H, J=5.5 Hz), 8.10 (d, 1H, J=7.5 Hz), 7.10-7.35 (m, 6H), 6.82 (d, 1H, J=7.5 Hz), 3.60-3.70 (m, 2H), 2.50-2.90 (m, 15H), 2.30-2.45 (m, 2H), 1.75-1.90 (m, 2H). LCMS (EI) m/z 390 (M+1).

Provenance & Evidence