HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butanoic acid, 4-chloro-4-oxo-, methyl ester → HCID 17962912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butanoic acid, 4-chloro-4-oxo-, methyl ester | HCID 73888 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 17962902 | HCID 17962902 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 17962912 | HCID 17962912 | — |
Reaction Steps
Acylation of 1-acetyl-6-(2-hydroxybenzoyl)amino-4-phenyl-1,2,3,4-tetrahydro-2,2,4-trimethylquinoline (20 mg) with 3-carbomethoxypropionyl chloride (14 mg) and N,N-diisopropylethylamine (40 μl) in tetrahydrofuran (2 ml) was performed according to the method described in example 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08258293B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-bf16aab756d743dbb5ba3d4096e555e3 |
| Source note | uspto-grants-2012_09 |